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The research carried out on the wall paintings of Hernán Pérez del Pulgar’s Palace chapel
in Granada (Spain) was aimed at determining its historical–artistic, stylistic, technical, and compositional
aspects. For this, a 16th century frieze and an 18th century pendentive were studied. The
mineralogical, chemical, and textural characterization of the constituent materials and the study of
the state of conservation of the paintings have helped to determine the pictorial technique used,
identify the nature of the salts present in the paintings, and other pathologies including a dormant
fungal attack. To this end, optical microscopy (OM), X-ray diffraction (XRD), Field emission scanning
electron microscopy with microanalysis (FESEM-EDS), and micro-Raman spectroscopy (MRS) were
used. The information obtained helps clarify important aspects of the painting technique used, laying
a basis to ensure effective and suitable conservation and restoration measures on the paintings that
will ensure their durability over time.Spanish Research Projects AERIMPACT (CGL2012-30729)
and EXPOAIR (P12-FQM-1889)The Andalusian Research Group RNM-179State Research Agency (SRA)Ministry of Science and Innovation under the
Research ProjectPID2020-119838RA-I0
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